N-CARBOBENZOXY-DL-VALINE

  • Name: N-CARBOBENZOXY-DL-VALINE
  • CAS: 3588-63-4
  • Purity: 99%
Inquiry

Details

N-CARBOBENZOXY-DL-VALINE GMP Manufacturer Global Trade 3588-63-4 with Fast Delivery

  • Molecular Formula: C13H17NO4
  • Molecular Weight: 251.282
  • Appearance/Colour: SOLID 
  • Melting Point: 78 °C 
  • Boiling Point: 432.6 °C at 760 mmHg 
  • Flash Point: 215.4 °C 
  • PSA： 75.63000 
  • Density: 1.182 g/cm3 
  • LogP: 2.41290 

N-CARBOBENZOXY-DL-VALINE(Cas 3588-63-4) Usage

InChI:InChI=1/C13H17NO4/c1-9(2)11(12(15)16)14-13(17)18-8-10-6-4-3-5-7-10/h3-7,9,11H,8H2,1-2H3,(H,14,17)(H,15,16)

3588-63-4 Relevant articles

Chiral tetraaryl-and tetraalkynylborates as chiral solvating agents for tetraalkylammonium salts

Tayama, Eiji,Sugawara, Takeshi

, p. 803 - 811 (2019/01/18)

The application of tetracarbon-substitut...

A Stereoselective entry into functionalized 1,2-diamines by zinc-mediated homologation of α-aminoacids

Hoang, Cam Thuy,Alezra, Valerie,Guillot, Regis,Kouklovsky, Cyrille

, p. 2521 - 2524 (2008/02/05)

A general, stereoselective synthsis of 4...

Asymmetric hydrogenation of N-sulfonylated-α-dehydroamino acids: Toward the synthesis of an anthrax lethal factor inhibitor

Shultz, C. Scott,Dreher, Spencer D.,Ikemoto, Norihiro,Williams, J. Michael,Grabowski, Edward J. J.,Krska, Shane W.,Sun, Yongkui,Dormer, Peter G.,DiMichele, Lisa

, p. 3405 - 3408 (2007/10/03)

(Chemical Equation Presented) A novel an...

Highly selective deprotection of tert-butyl esters using ytterbium triflate as a catalyst under mild conditions

Sridhar, P. Ramu,Sinha, Surajit,Chandrasekaran

, p. 157 - 160 (2007/10/03)

Ytterbium triflate catalyses the deprote...

3588-63-4 Process route

D,L-valine
516-06-3,25609-85-2,7004-03-7,921-10-8

D,L-valine

benzyl chloroformate
501-53-1,94274-21-2

benzyl chloroformate

N-benzyloxycarbonylvaline
1149-26-4,1685-33-2,92077-76-4,3588-63-4

N-benzyloxycarbonylvaline

Conditions
Conditions Yield
With sodium hydroxide; In water; 0 deg C to r.t., 1 h;
82%
With sodium hydroxide; In water;
60%
With sodium hydroxide; at 20 ℃; for 15h;
With sodium hydroxide; N-ethyl-N,N-diisopropylamine; In acetone; at 0 - 20 ℃;
With sodium hydrogencarbonate; In water;
With sodium hydroxide; In water; at 0 - 20 ℃; for 3.5h;
tert-butyl 2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate
20314-88-9

tert-butyl 2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate

N-benzyloxycarbonylvaline
1149-26-4,1685-33-2,92077-76-4,3588-63-4

N-benzyloxycarbonylvaline

Conditions
Conditions Yield
With ytterbium(III) triflate; In nitromethane; at 45 - 50 ℃; for 5h;
97%

3588-63-4 Upstream products

  • 516-06-3
    516-06-3

    D,L-valine

  • 501-53-1
    501-53-1

    benzyl chloroformate

  • 91806-74-5
    91806-74-5

    3,5-dimethyl-pyrazole-1-carboxylic acid benzyl ester

  • 20314-88-9
    20314-88-9

    tert-butyl 2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate

3588-63-4 Downstream products

  • 134306-34-6
    134306-34-6

    N-(Benzyloxycarbonyl)valine methyl ester

  • 4108-18-3
    4108-18-3

    N -benzyloxycarbonyl-valine 4-nitro-phenyl ester

  • 879123-73-6
    879123-73-6

    N -(N -benzyloxycarbonyl-valyl)-alanine ethyl ester

  • 105120-38-5
    105120-38-5

    N -(N -benzyloxycarbonyl-valyl)-phenylalanine ethyl ester

Related Products